2-Aminomethyl-1-ethylpyrrolidine → HCID 54214393, compound

HRID 1637611Notes

Reaction equation

HRID 1637611 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[C:10]([O:18][CH3:19])[C:11]=1[O:12][CH2:13][CH:14]=[C:15]([CH3:17])[CH3:16])[C:6]([OH:8])=O.[NH2:20][CH2:21][CH:22]1[CH2:26][CH2:25][CH2:24][N:23]1[CH2:27][CH3:28]>>[CH2:27]([N:23]1[CH2:24][CH2:25][CH2:26][CH:22]1[CH2:21][NH:20][C:6](=[O:8])[C:5]1[CH:9]=[C:10]([O:18][CH3:19])[C:11]([O:12][CH2:13][CH:14]=[C:15]([CH3:17])[CH3:16])=[C:3]([O:2][CH3:1])[CH:4]=1)[CH3:28]

Participants

3

Reactant 2

HCID 1172952-Aminomethyl-1-ethylpyrrolidineHCID 18799460HCID 18799460, compound

Product 1

HCID 54214393HCID 54214393, compoundYield 89.3%

Procedure

In a manner identical to Example 15, 3,5-dimethoxy-4-prenyloxybenzoic acid (0.80 g) was subjected to a condensation reaction with 2-aminomethyl-1-ethylpyrrolidine (0.39 g), thereby yielding 1.01 g(89%) of the aimed compound.

Sources & evidence

ORD record
ord-a60e044d4f6640c09a8b82fea1938faf
Source dataset
uspto-grants-2000_03
Patent number
US06043243

Reaction notes

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