HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 1-methoxy-4-(2-nitroethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 4-Methoxy-beta-nitrostyrene | HCID 229843 | — |
| Product | 1-methoxy-4-(2-nitroethyl)benzene | HCID 487892 | 93% |
Reaction Steps
227 A) 4-Methoxy-b-nitrostyrene (25.0 g, 0.15 mole) was reacted with benzaldehyde (19.1 g, 0.18 mole) and 1,2-diaminobenzene (19.8 g, 0.18 mole) according to the procedure of Chikashita et. al. (Synth. Commun. 1985, 15 (6), 527) to yield methoxy-4-(2-nitroethyl)benzene (25.0 g, 93%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043261 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-386ed8b34f9441278cc9fbd1318e43d5 |
| Source note | uspto-grants-2000_03 |