HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 53749415, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Ammonium Persulfate | HCID 62648 | — |
| Reactant | HCID 12539734 | HCID 12539734 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53749415 | HCID 53749415 | 29% |
Reaction Steps
Treatment of 4-(N,N-diethylaminomethyl)pyridine (2.0 g, 12.20 mmol) with ammonium persulfate (5.56 g, 24.4 g, 2.0 equiv.), methanol (22 ml), water (11 ml) and concentrated H2SO4 (2.76 g, 28.18 mmol, 2.31 equiv.) as described for Cpd #214 gave 0.697 g (29%) of 4-(N,N-diethylaminomethyl)-2-hydroxymethylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043248 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-861ebefcc98f4d0fa5e07b075a2202c4 |
| Source note | uspto-grants-2000_03 |