HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tryptamine → HCID 22256590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tryptamine | HCID 1150 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Methyl 4-Formylbenzoate | HCID 15294 | — |
| Product | HCID 22256590 | HCID 22256590 | 9.4% |
Reaction Steps
This product was prepared using the same procedure as for Intermediate 1 with tryptamine (2.8 g, 17.4 mmol), 4-formylbenzoic acid, methyl ester (2.87 g, 1.1 equiv.) and TFA (2.7 mL, 2 equiv.) to give the title compound (0.5 g, 9%) as white crystals after recrystallization from isopropanol:H2O. MP: 179° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043252 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-34bb69520db54d29a69a9021ce3030f4 |
| Source note | uspto-grants-2000_03 |