HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cuminaldehyde → HCID 3583733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cuminaldehyde | HCID 326 | — |
| Reactant | Tryptamine | HCID 1150 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 3583733 | HCID 3583733 | 67% |
Reaction Steps
This product was prepared using the same procedure as for Intermediate 1 with tryptamine (5.0 g, 31.2 mmol), 4-isopropylbenzaldehyde (5.08 g, 1.1 equiv.) and TFA (4.8 mL, 2 equiv.) to give the title compound (5.9 g, 67%) as white crystals after recrystallization from iPr2O. MP: 146° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043252 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-c9d88a1d92f34412942c31f78e9b6b6e |
| Source note | uspto-grants-2000_03 |