HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → (E)-3-[4-(3-Dimethylaminopropenyl)phenyl]acrylic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | (E)-3-[4-(3-dimethylaminopropenyl)phenyl]acrylic acid, methyl ester | HCID 86755260 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (E)-3-[4-(3-Dimethylaminopropenyl)phenyl]acrylic Acid | HCID 70098974 | 85% |
Reaction Steps
This product was prepared by refluxing for four hours, (E)-3-[4-(3-dimethylaminopropenyl)phenyl]acrylic acid, methyl ester with NaOH (0.16 g, 2 equiv.) in 10 mL of MeOH. After evaporation of the solvent in vacuo, treatment with 5 mL of HCl (1N) gave the title compound (0.4 g, 85%) as a gummy orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043252 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-5f1af7ce008f423e87cf0593116f4905 |
| Source note | uspto-grants-2000_03 |