HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 70109926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 87228647 | HCID 87228647 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70109926 | HCID 70109926 | 90% |
Reaction Steps
A stirred solution of Example 23 (0.5 g, 1.0 mmol) in MeOH was refluxed with methylamine (1.6 mL, 1.5 equiv., 33% in EtOH) for one hour. Evaporation in vacuo gave (E)-1-[1-(3,4-methylenedioxyphenyl)-1,3,4,9-tetrahydro-β-carbolin-2-yl]-3-(4-methyliminomethylphenyl)propene-1-one (0.46 g, 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043252 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-133d5896e7c745b2bcf8dc43b3861734 |
| Source note | uspto-grants-2000_03 |