HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178517272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Imidazol-1-ylmethylphenylamine | HCID 1265319 | — |
| Reactant | 3-(1-Ethoxy-1-phenylmethylidene)-5-nitro-2-indolinone | HCID 53734887 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178517272 | HCID 178517272 | 90% |
Reaction Steps
Prepared from 3-{1-ethoxy-1-phenylmethylidene}-5-nitro-2-indolinone and 1.5 equivalents of 4-(imidazol-1-yl)methyl-aniline (melting point: 128-130° C.) in DMF (120° C., 1 hour), pouring into water and washing the precipitate with MeOH and ether. Yield: 90% of theory;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043254 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-9376af469e7143f58656c880d8270ca0 |
| Source note | uspto-grants-2000_03 |