Nitric Acid → HCID 178526603, compound

HRID 1637947Notes

Reaction equation

HRID 1637947 reaction equation
[CH2:1]([C:8]1[N:9]=[CH:10][NH:11][CH:12]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+:13]([O-])([OH:15])=[O:14]>>[N+:13]([C:5]1[CH:4]=[CH:3][C:2]([CH2:1][C:8]2[N:9]=[CH:10][NH:11][CH:12]=2)=[CH:7][CH:6]=1)([O-:15])=[O:14]

Participants

3

Reactant 2

HCID 944Nitric AcidHCID 178420208HCID 178420208, compound

Product 1

HCID 178526603HCID 178526603, compound

Procedure

Prepared according to Arch. Pharm. 1975, 308, 755-759 by reacting 4-benzyl-1H-imidazole in fuming 100% nitric acid at -10 to -5° C. (30 minutes).

Workup

  1. customPrepared
  2. customat -10 to -5° C.
  3. custom(30 minutes)

Sources & evidence

ORD record
ord-e276872af3464087ae507e1354c8ae6a
Source dataset
uspto-grants-2000_03
Patent number
US06043254

Reaction notes

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