Bromocyclopentane → HCID 18801197, compound

HRID 1638200Notes

Reaction equation

[ClH:1].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)[CH2:18][NH:17][C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.Br[CH:30]1[CH2:34][CH2:33][CH2:32][CH2:31]1>>[ClH:1].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)[CH2:18][N:17]([CH:30]4[CH2:34][CH2:33][CH2:32][CH2:31]4)[C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

Reactant 2

HCID 8728Bromocyclopentane

HCID 19347388HCID 19347388, compound

Product 1

HCID 18801197HCID 18801197, compound

Procedure

The title compound, white solid, m. p. 221° C. and MS: m/e=438.3 (M+H+) was prepared in accordance with the general method of example 24 from 8-cyclodecyl-1-phenyl-1,3,8-triaza-spiro[4,5]decan-4-one hydrochloride and bromocyclopentane.

Sources & evidence

ORD record: ord-dcff3b709ec14fdf96017fce9039b333
Source dataset: uspto-grants-2000_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06043366

Reaction notes

Loading…