2-(2-Bromoethyl)-1,3-dioxolane → HCID 19347351, compound

HRID 1638205Notes

Reaction equation

HRID 1638205 reaction equation
[ClH:1].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)[CH2:18][NH:17][C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.Br[CH2:30][CH2:31][CH:32]1[O:36][CH2:35][CH2:34][O:33]1>>[ClH:1].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)[CH2:18][N:17]([CH2:30][CH2:31][CH:32]4[O:36][CH2:35][CH2:34][O:33]4)[C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 877762-(2-Bromoethyl)-1,3-dioxolaneHCID 19347388HCID 19347388, compound

Product 1

HCID 19347351HCID 19347351, compound

Procedure

The title compound, white solid, m. p. 205° C. and MS: m/e=470.6 (M+H+) was prepared in accordance with the general method of example 24 from 8-cyclodecyl-1-phenyl-1,3,8-triaza-spiro[4,5]decan-4-one hydrochloride and 2-(2-bromoethyl)-1,3-dioxolane.

Sources & evidence

ORD record
ord-b7dc1be823c44883ac29f34b9ded4637
Source dataset
uspto-grants-2000_03
Patent number
US06043366

Reaction notes

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