2-(5-Methyl-2-phenyl-1,3-oxazol-4-yl)ethyl methanesulfonate → HCID 19347367, compound
Reaction equation
[ClH:1].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)[CH2:18][NH:17][C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[CH3:29][C:30]1[O:34][C:33]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)=[N:32][C:31]=1[CH2:41][CH2:42]OS(C)(=O)=O>>[ClH:1].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)[CH2:18][N:17]([CH2:42][CH2:41][C:31]4[N:32]=[C:33]([C:35]5[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=5)[O:34][C:30]=4[CH3:29])[C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1Participants
3
Procedure
The title compound, white solid, m. p. 140° C. and MS: m/e=555.3 (M+H+) was prepared in accordance with the general method of example 24 from 8-cyclodecyl-1-phenyl-1,3,8-triaza-spiro[4,5]decan-4-one hydrochloride and methanesulfonic acid 2-(5-methyl-2-phenyloxazol-4-yl)-ethyl ester.
Sources & evidence
- ORD record
- ord-e9ce6ea0b51c46c88590ebdd25ccf290
- Source dataset
- uspto-grants-2000_03
- Patent number
- US06043366
Reaction notes
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