2-chloro-N,N-dimethylacetamide → HCID 19347386, compound

HRID 1638210Notes

Reaction equation

HRID 1638210 reaction equation
Cl.[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)[CH2:18][NH:17][C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[CH3:29][N:30]([CH3:35])[C:31](=[O:34])[CH2:32][Cl:33]>>[ClH:33].[CH:2]1([N:12]2[CH2:28][CH2:27][C:15]3([N:19]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)[CH2:18][N:17]([CH2:32][C:31]([N:30]([CH3:35])[CH3:29])=[O:34])[C:16]3=[O:26])[CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 758862-chloro-N,N-dimethylacetamideHCID 19347388HCID 19347388, compound

Product 1

HCID 19347386HCID 19347386, compound

Procedure

The title compound, white solid, m. p. 145° C. and MS: m/e=455.6 (M+H+) was prepared in accordance with the general method of example 24 from 8-cyclodecyl-1-phenyl-1,3,8-triaza-spiro[4,5]decan-4-one hydrochloride and N,N-dimethyl-2-chioroacetamide.

Sources & evidence

ORD record
ord-6c105da5dcae426abace1266f6e53779
Source dataset
uspto-grants-2000_03
Patent number
US06043366

Reaction notes

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