Water → HCID 19788753, compound

Participants

Reaction Steps

2-Hexyldecanoyl chloride (25 g) was added during 10 minutes to a stirred solution of 1,2,4-triazole (14 g) and pyridine (10 ml) in acetone (50 ml). During addition the temperature rose from 20° to 38°. The mixture was drowned into water and extracted with toluene, and the toluene solution was washed with water and then distilled yielding 1-(2'-hexyldecanoyl)-1,2,4-triazole (33 g), b.p. 156°-160° at 0.15 mm of mercury. This compound was evaluated as an extractant for copper using the procedure of Example 1 and the results are presented in Table 1.

Provenance & Evidence