HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 12777162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 3-Chlorodiphenylamine | HCID 7545 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12777162 | HCID 12777162 | — |
Reaction Steps
N-(3-Chlorophenyl)aniline (25.1 g, 0.123 mole) and chloroacetyl chloride (19.6 ml, 0.246 mole) were refluxed in toluene (100 ml) for 4 hours, then stripped of toluene and excess acid chloride in vacuo to yield an oil which crystallized on scratching. Recrystallization from ethanol/H2O gave purified title product, 32.6 g, m.p. 94°-96.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04879391 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-94e2bb9448f943a98ae3ed2ccac219d8 |
| Source note | uspto-grants-1989_11 |