HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl (o-nitrobenzylthio)-acetate → HCID 43617941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl (o-nitrobenzylthio)-acetate | HCID 12136843 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 43617941 | HCID 43617941 | — |
Reaction Steps
Methyl (o-nitrobenzylthio)-acetate (24.4 g) was dissolved in ethanol (500 ml). Raney nickel was added and the mixture was hydrogenated at room temperature and 1 atm. of hydrogen pressure. The title compound was obtained as an oil after filtration and evaporation of the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04880799 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-54086d2128b74a24a295281473238772 |
| Source note | uspto-grants-1989_11 |