HRID1638729

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6093208

未命名化合物

$结构：CC1=C(CC(=O)O)c2cc(F)ccc2/C1=C\c1ccc([S+](C)[O-])cc1$

HCID178427217

未命名化合物

PRODUCTS

生成物

$结构：CC1=C(CC(=O)O)c2cc(F)ccc2/C1=C\c1ccc([S+](C)[O-])cc1.[Ca]$

HCID178427218

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

100 g Sulindac is suspended in 4 l. of 75% v/v ethanol. Apply heat until a clear solution is formed. Add 10.38 g of calcium hydroxide and mix. A clear solution is formed initially followed by massive precipitation of calcium sulindac. Filter the slurry to remove the solvent and air dry to give calcium sulindac.

WORKUP

后处理

temperatureApply heat until a clear solution
customis formed
additionmix
customA clear solution is formed initially
customfollowed by massive precipitation of calcium sulindac
filtrationFilter the slurry
customto remove the solvent and air
customdry