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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1638773Generated: October 26, 2026

1,2-Bis(2-chloroethoxy)ethane → 1,8-Bis[(2-pyridyl)(phenyl)phosphino]-3,6-dioxaoctane

https://huagongshe.com/reaction/1638773

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2-Bis(2-chloroethoxy)ethaneHCID 8171—
ReactantBis[(2-pyridyl)(phenyl)phosphino]methaneHCID 22163400—
SolventDichloromethaneHCID 6344—
Product1,8-Bis[(2-pyridyl)(phenyl)phosphino]-3,6-dioxaoctaneHCID 19803149—

Reaction Steps

Some 1,8-bis[(2-pyridyl)(phenyl)phosphino]-3,6-dioxaoctane was prepared substantially in the same way as the diphosphine of Example 2, except that instead of dichloromethane, 1,8-dichloro-3,6-dioxaoctane was employed.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04880902
Source datasetuspto-grants-1989_11
ORD IDord-788815406d844d02804dd38419d40b27
Source noteuspto-grants-1989_11