HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,7-Dimethoxy-2-naphthoic acid → HCID 14676175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,7-Dimethoxy-2-naphthoic acid | HCID 283028 | — |
| Reactant | 1-(3,4,5-Trimethoxybenzoyl)piperazine | HCID 2874204 | — |
| Product | HCID 14676175 | HCID 14676175 | — |
Reaction Steps
In a manner as that described in Example 62, 6,7-dimethoxy-2-naphthoic acid and 1-(3,4,5-trimethoxybenzoyl)piperazine are subjected to amidation to give 1-(6,7-dimethoxy-2-naphthoyl)-4-(3,4,5-trimethoxybenzoyl)piperazine. This product is recrystallized from ethyl acetate to give colorless needles, m.p. 224°-226° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04880809 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-51df90c591be4aafad0cba5ecd5912ba |
| Source note | uspto-grants-1989_11 |