Thionyl Chloride → HCID 54019687, compound

HRID 1638952Notes

Reaction equation

HRID 1638952 reaction equation
[CH2:1]([O:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:13]=1[C:24]([OH:26])=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].O=S(Cl)[Cl:29]>>[CH2:1]([O:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:13]=1[C:24]([Cl:29])=[O:26])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 19898360HCID 19898360, compound

Product 1

HCID 54019687HCID 54019687, compound

Procedure

20 ml of SOCl2 was added to 4 g (1.13×10-2 mol) of decyloxybiphenylcarboxylic acid, and the mixture was heated at reflux for 3.5 hours. Excessive SOCl2 was evaporated to obtain decyloxybiphenylcarboxylic acid chloride.

Workup

  1. temperaturethe mixture was heated
  2. temperatureat reflux for 3.5 hours
  3. customExcessive SOCl2 was evaporated

Sources & evidence

ORD record
ord-cd70575773804eb288bbcd684660b955
Source dataset
uspto-grants-1989_11
Patent number
US04882085

Reaction notes

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