HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octanol → HCID 15696565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octanol | HCID 957 | — |
| Reactant | 5-Hydroxy-2-pyrrolidone | HCID 194148 | — |
| Product | HCID 15696565 | HCID 15696565 | — |
Reaction Steps
7.5 g of 5-hydroxy-pyrrolidin-2-one, 10 cm3 of n-octanol and 4 g of Amberlite IR 120H are heated to 60° C. for 4 hours. After filtering, the n-octanol is eliminated by distilling under reduced pressure. 5.5 g of the expected product is obtained, m.p. 36°-38° C., crystallized from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04882350 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-1f5cd7c854d64e72960378e2514498cf |
| Source note | uspto-grants-1989_11 |