4'-Hydroxyacetophenone → HCID 13120356, compound

HRID 1639067Notes

Reaction equation

HRID 1639067 reaction equation
Cl[CH2:2][CH:3]([OH:7])[CH2:4][CH2:5][Cl:6].[CH3:8][C:9]([C:11]1[CH:12]=[CH:13][C:14]([OH:17])=[CH:15][CH:16]=1)=[O:10]>C(O)C.C(OCC)C>[Cl:6][CH2:5][CH2:4][CH:3]([OH:7])[CH2:2][O:17][C:14]1[CH:15]=[CH:16][C:11]([C:9](=[O:10])[CH3:8])=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 74694'-HydroxyacetophenoneHCID 170211,4-Dichloro-2-butanol

Product 1

HCID 13120356HCID 13120356, compound

Reagents, catalysts & solvents 1

HCID 21585056Diethyl ether ethanolSolvent

Procedure

Utilizing the procedure of Preparation 16, 1,4-dichloro-2-butanol was reacted with 4-hydroxyacetophenone to give cream colored solid, m.p. 75°-77° C. Recrystallizing solvent was a mixture of ethanol-diethyl ether.

Workup

  1. customto give cream colored solid, m.p. 75°-77° C

Sources & evidence

ORD record
ord-c80edcace9ff423d8edd7733e42ecd28
Source dataset
uspto-grants-1989_11
Patent number
US04882330

Reaction notes

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