Potassium Iodide → HCID 14422897, compound

Participants

Reaction Steps

This compound was prepared according to the procedure of Example 25. A mixture of 8.1 g (0.03 mole) of 4-chloro-1-(3,4-dichlorophenoxy)-2-butanol, 4.9 g (0.03 mole) of 1-phenylpiperazine, 16.0 g (0.15 mole) of anhydrous sodium carbonate and 0.3 g (0.002 mole) of potassium iodide in a total volume of 200 ml of 1-butanol gave a golden oil as residue. The hydrochloric acid salt was formed in ethereal hydrogen chloride and the collected solid was recrysrallized from methanol-ethyl ether to give 5.1 g (37%) of white solid, m.p. 210°-213° C.

Provenance & Evidence