HCID 19840246, compound → HCID 19840252, compound
Reaction equation
[O:1]([CH2:8][CH:9]([OH:27])[CH2:10][CH2:11][N:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:23]=[CH:22][C:21]([N+:24]([O-])=O)=[CH:20][CH:19]=2)[CH2:14][CH2:13]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[H][H]>[Pd]>[O:1]([CH2:8][CH:9]([OH:27])[CH2:10][CH2:11][N:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:19]=[CH:20][C:21]([NH2:24])=[CH:22][CH:23]=2)[CH2:14][CH2:13]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The title compound is prepared by catalytic reduction of 1-phenoxy-4-[4-(4-nitrophenyl)-1-piperazinyl]-2-butanol with hydrogen over palladium on carbon.
Sources & evidence
- ORD record
- ord-97e18ae2db9d4beb8add4af5d793d858
- Source dataset
- uspto-grants-1989_11
- Patent number
- US04882330
Reaction notes
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