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3-Isopropoxy-4-nitrotoluene → 4-Methyl-2-(propan-2-yloxy)aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Isopropoxy-4-nitrotoluene | HCID 592731 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-Methyl-2-(propan-2-yloxy)aniline | HCID 15068114 | — |
反応手順
5-Methyl-1-(1-methylethoxy)-2-nitrobenzene, 17.7 g (91 mmol), is dissolved in methanol, palladium on charcoal is added and the mixture is exposed to hydrogen gas until the required amount of hydrogen is absorbed. The mixture is worked up in the usual manner to give 15 g of 4-methyl-2-(1-methylethoxy)benzenamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04882357 |
| 出典データセット | uspto-grants-1989_11 |
| ORD ID | ord-3e627e157205460095844073242a2bc9 |
| 出典メモ | uspto-grants-1989_11 |