(-)-Carnitine → HCID 131716200, compound

HRID 1639224Notes

Reaction equation

HRID 1639224 reaction equation
[CH3:1][N+:2]([CH2:5][C@H:6]([OH:11])[CH2:7][C:8]([O-:10])=[O:9])([CH3:4])[CH3:3].[NH2:12][C@H:13]([C:18]([O-:20])=[O:19])[CH2:14][C:15]([O-:17])=[O:16].[K+:21].[K+]>O>[NH2:12][C@H:13]([C:18]([O-:20])=[O:19])[CH2:14][C:15]([O-:17])=[O:16].[K+:21].[OH:11][C@H:6]([CH2:7][C:8](=[O:9])[O-:10])[CH2:5][N+:2]([CH3:4])([CH3:1])[CH3:3].[K+:21]

Participants

4

Reactant 2

HCID 10917(-)-CarnitineHCID 6454950Aspartic acid, potassium salt

Product 1

HCID 131716200HCID 131716200, compoundYield 218.5%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

An amount of 16.21 g of L-carnitine inner salt is dissolved in 30 ml of water; 17.32 g of potassium aspartate dissolved in 10 ml of water are added. The mixture is stirred up to complete dissolution. The solution is submitted to freeze drying; 33.5 g of L-carnitine potassium aspartate are obtained; the spectroscopic analyses confirm its structure.

Workup

  1. additionare added
  2. dissolutiondissolution
  3. customto freeze drying

Sources & evidence

ORD record
ord-c1b518ab7e1a4abb8aadfafa3fdcb167
Source dataset
uspto-grants-1989_11
Patent number
US04883786

Reaction notes

Loading…