HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3760131, compound → HCID 1787923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3760131 | HCID 3760131 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 1787923 | HCID 1787923 | 98.2% |
Reaction Steps
22.0 g (0.1 mole) of methyl 3-(β-phenylacryloyl)-carbazate are dissolved in 300 ml. of methanol and the solution is hydrogenated in the presence of 0.2 g. of a palladium-charcoal catalyst. The solution is evaporated. Thus 21.8 g of the white crystalline desired compound are obtained. Yield: 98.2%. M.p.: 118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04883907 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-6988742cf2144b8e85ad210f21489b97 |
| Source note | uspto-grants-1989_11 |