Propionic Acid → Palladium(II) propionate

HRID 1639478Notes

Reaction equation

HRID 1639478 reaction equation
CC(O)=O.CC(O)=O.[Pd:9].[C:10]([OH:14])(=[O:13])[CH2:11][CH3:12]>>[C:10]([O-:14])(=[O:13])[CH2:11][CH3:12].[Pd+2:9].[C:10]([O-:14])(=[O:13])[CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 1032Propionic AcidHCID 4144353Palladium (II) acetate

Product 1

HCID 11459426Palladium(II) propionate

Procedure

5 gm commercial palladium(II) acetate trimer (Aldrich) was added to 40 g of propionic acid. The mixture was maintained at 40 degrees Celsius for 24 hours. Excess propionic acid was removed under vacuum at room temperature. The resulting yellow solid was used for making palladium inks.

Workup

  1. temperatureThe mixture was maintained at 40 degrees Celsius for 24 hours
  2. customExcess propionic acid was removed under vacuum at room temperature

Sources & evidence

ORD record
ord-7d7570892ebf418f905cbd5615a71312
Source dataset
uspto-grants-2012_02
Patent number
US08110254B1

Reaction notes

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