HRID1639515

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID17022

Benzaldehyde, 3-chloro-4-hydroxy- (8CI)(9CI)

C7H5ClO2

结构：CS(=O)(=O)OC1CN(C(=O)c2nnc(-c3ccccc3)o2)C1

HCID58043099

未命名化合物

PRODUCTS

生成物

结构：O=Cc1ccc(OC2CN(C(=O)c3nnc(-c4ccccc4)o3)C2)c(Cl)c1

HCID58043128

未命名化合物

收率 34.5%

PROCEDURE

实验过程

Using a similar protocol as described in Example 9A but employing 1C (500 mg, 1.55 mmol) and 3-chloro-4-hydroxybenzaldehyde (250 mg, 1.60 mmol) as starting materials gave 205 mg (34%) of 10A as a solid. 1H NMR (500 MHz, CD3OD): δ 4.33 (m, 1H), 4.6-4.9 (m, 2H), 5.23 (m, 1H), 5.36 (m, 1H), 7.07 (d, 1H), 7.5-7.7 (m, 3H), 7.8-9.0 (m, 4H), 9.86 (s, 1H).