Benzene → Cumene

HRID 1640080Notes

Reaction equation

HRID 1640080 reaction equation
[CH2:1]=[CH:2][CH3:3].[CH:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>>[C:4]1([CH:2]([CH3:3])[CH3:1])[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 241BenzeneHCID 8252Propylene4×

Product 1

HCID 7406Cumene

Procedure

A 75 ml Hoke transfer vessel was then filled with 28.1 grams of liquid propylene and connected to the reactor vessel, and then connected with 2169 kPa-a ultra high purity nitrogen. After the one-hour benzene stir time had elapsed, the propylene was transferred from the Hoke vessel to the reactor. The 2169 kPa-a nitrogen source was maintained connected to the propylene vessel and open to the reactor during the entire run to maintain constant reaction pressure during the test. Liquid product samples were taken at 30, 60, 120, 150, 180 and 240 minutes after addition of the propylene.

Workup

  1. temperatureThe 2169 kPa-a nitrogen source was maintained
  2. temperatureto maintain constant
  3. customreaction pressure during the test
  4. customwere taken at 30, 60, 120, 150, 180 and 240 minutes

Sources & evidence

ORD record
ord-7841d94416354b369f4cc6eb0edd0445
Source dataset
uspto-grants-2012_02
Patent number
US08110715B2

Reaction notes

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