5-Bromo-3-methoxyquinoline → HCID 87130306, compound

Participants

Reaction Steps

This aldehyde was prepared using sequentially the protocols of Example 29, step 29.i and Example 33, steps 33.i to 33.ii and starting from 5-bromo-3-methoxy-quinoline (4 g, 16.7 mmol; prepared as in DE 10316081). After chromatography on SiO2 (Hex/EA 1:1, EA), the compound was obtained as a yellowish solid (0.95 g, 30% yield over 3 steps).

Provenance & Evidence