HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanamide → HCID 59553234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanamide | HCID 9864 | — |
| Reactant | 3-fluoro-N-(4-{[2-(methylsulfonyl)pyrimidin-4-yl]oxy}-1-naphthyl)-5-morpholin-4-ylbenzamide | HCID 59553095 | — |
| Product | HCID 59553234 | HCID 59553234 | — |
Reaction Steps
Compound is prepared from 3-fluoro-N-(4-{[2-(methylsulfonyl)pyrimidin-4-yl]oxy}-1-naphthyl)-5-morpholin-4-ylbenzamide and cyanamide according to conditions described in general procedure C. 1H NMR (400 MHz, CDCl3) δ 3.21 (t, J=4.8 Hz, 4 H), 3.81 (t, J=5.2 Hz, 4 H), 6.34 (d, J=6.0 Hz, 1 H), 6.70 (d, J=12.0 Hz, 1H), 7.16-7.20 (m, 2 H), 7.32-7.46 (m, 4 H), 7.76-7.78 (s, 1 H), 7.86-7.89 (m 1 H), 8.05 (d, J=6.4 Hz, 1 H), 9.61 (s, 1 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08114873B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-d641ee3379f844449af4e9927529e205 |
| Source note | uspto-grants-2012_02 |