Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1641483Generated: November 1, 2026

Heptane → HCID 46830963, compound

https://huagongshe.com/reaction/1641483

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHeptaneHCID 8900—
ReactantHCID 46830960HCID 46830960—
SolventEthyl AcetateHCID 8857—
ProductHCID 46830963HCID 4683096380.2%

Reaction Conditions

Temperature0 °C

Reaction Steps

The compound (50 mg) prepared in Example 14 (3) was dissolved in ethyl acetate (1.4 mL) at 70° C. To the solution, n-heptane (0.68 mL) was added at room temperature, which was then cooled to 0° C. The precipitated solid was filtered and dried under reduced pressure to obtain the title compound (39 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08115014B2
Source datasetuspto-grants-2012_02
ORD IDord-9b528aa5fcca4ee2b141c8dc5d7b0f9e
Source noteuspto-grants-2012_02