Ethanol → HCID 44468077, compound

Participants

Reaction Steps

The title compound was prepared from Intermediate 4 (400 mg, 1.4 mmol), (3-methoxy-2-pentyloxy)benzaldehyde (498 mg, 2.22 mmol) and sodium ethoxide (190 mg, 2.8 mmol) in ethanol (25 ml) according to procedure described in Example 9 to give 300 mg of the product as a light yellow solid; 1H NMR (300 MHz, DMSO-d6) δ 0.90-1.00 (m, 3H), 1.25-1.45 (m, 4H), 1.46-1.60 (m, 2H), 3.77 (s, 3H), 3.65-3.85 (m, 2H), 6.87 (d, J=16.2 Hz, 1H), 6.96-7.00 (m, 3H), 7.54-7.57 (m, 3H), 7.93 (d, J=7.5 Hz, 1H), 8.00-8.01 (m, 2H), 8.09 (d, J=14.7 Hz, 1H); ESI-MS (m/z) 472.27 (M+H)+.

Provenance & Evidence