HCID 58880053, compound → HCID 58880126, compound

Participants

Reaction Steps

The title compound was synthesized from Compound 157 using an analogous procedure to that outlined in the preparation of Compound 211. 1H NMR (400 MHz, DMSO-d6) δ ppm 1.17 (t, J=7.45 Hz, 3 H) 1.36 (d, J=6.06 Hz, 3 H) 2.26 (s, 3 H) 3.40 (q, J=7.41 Hz, 2 H) 3.63-3.72 (m, 2 H) 4.63 (m, 1 H) 4.90 (t, J=6.19 Hz, 1 H) 7.07 (d, J=8.08 Hz, 1 H) 7.15-7.19 (m, 1 H) 7.56 (s, 1 H) 7.85 (t, J=7.71 Hz, 1 H) 7.97-7.99 (m, 2 H) 8.07-8.10 (m, 1 H) 8.27 (d, J=2.02 Hz, 1 H) 11.82 (s, 1 H); [M+H] calc'd for C23H25N2O4S, 425.2.; found, 425.3.

Provenance & Evidence