HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-ol → HCID 58880180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-ol | HCID 58880081 | — |
| Reactant | 3-chloro-5-(3-(ethylsulfonyl)phenyl)-8-methoxy-9H-pyrido[2,3-b]indol-8-ol | HCID 86612633 | — |
| Product | HCID 58880180 | HCID 58880180 | — |
Reaction Steps
The title compound was prepared from Compound 217 by using an analogous procedure to that outlined in the preparation of Compound 157. 1H NMR (400 MHz, Methanol-d4) δ 8.35 (s, 1 H) 8.15(m, 1 H) 8.07 (m, 1 H) 7.97 (m, 1 H) 7.88 (t, J=8.0 Hz, 1 H) 7.66 (s, 1 H) 7.23 (d, J=8.36 Hz, 1 H) 7.16 (d, J=8.36 Hz, 1 H) 4.44 (t, J=5.8 Hz, 2 H) 3.72 (t, J=8.0 Hz, 2 H) 3.43 (q, J=7.32 Hz, 2 H) 3.03 (s, 6 H) 2.41 (m, 2 H) 1.34 (t, J=7.32 Hz, 3 H) [M+H] calc'd for C24H27ClN3O3S, 472; found, 472.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119655B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-7fccdeae55f740a89546bb23a6efa0b2 |
| Source note | uspto-grants-2012_02 |