HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58880180, compound → HCID 58880108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58880180 | HCID 58880180 | — |
| Reactant | 3-(5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-yloxy)-N,N-dimethylpropan-1-amine | HCID 58880181 | — |
| Product | HCID 58880108 | HCID 58880108 | — |
Reaction Steps
The title compound was prepared from Compound 218 by using an analogous procedure to that outlined in the preparation of Compound 205. 1H NMR (400 MHz, Methanol-d4) δ 8.40 (s, 1 H) 8.14 (m, 1 H) 8.10 (m, 1 H) 8.00 (m, 1 H) 7.89 (t, J=8.0 Hz, 1 H) 7.69 (s, 1 H) 7.28 (d, J=8.08 Hz, 1 H) 7.20 (d, J=8.08 Hz, 1 H) 4.68 (t, J=5.0 Hz, 2 H) 3.80 (t, J=5.0 Hz, 2 H) 3.43 (q, J=7.32 Hz, 2 H) 3.13 (s, 6 H) 1.33 (t, J=7.32 Hz, 3 H). [M+H] calc'd for C23H25ClN3O3S, 458; found, 458.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119655B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-087d3f258e134aafa6a520bb8e1d519d |
| Source note | uspto-grants-2012_02 |