HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-ol → HCID 58880071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-ol | HCID 58880081 | — |
| Reactant | HCID 58880155 | HCID 58880155 | — |
| Product | HCID 58880071 | HCID 58880071 | — |
Reaction Steps
The title compound was prepared from Compound 157 using an analogous procedure to the procedure described for the preparation of Compound 233. 1H NMR (400 MHz, DMSO-d6) δ ppm 1.17 (t, J=7.33 Hz, 3 H) 1.25 (d, J=6.06 Hz, 3 H) 2.27 (s, 3 H) 3.41 (q, J=7.33 Hz, 2 H) 3.94 (m, 1 H) 4.09-4.16 (m, 2 H) 4.97 (d, J=4.04 Hz, 1 H) 7.07-7.14 (m, 2 H) 7.57 (s, 1 H) 7.85 (t, J=7.71 Hz, 1 H) 7.96-8.00 (m, 2 H) 8.09 (s, 1 H) 8.28 (d, J=1.52 Hz, 1 H) 11.94 (s, 1 H); [M+H] calc'd for C23H25N2O4S, 425.2; found, 425.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119655B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-6b13ca96f4014ef6860ab3a3c8439fd6 |
| Source note | uspto-grants-2012_02 |