HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N-Hydroxy-6-methyl-nicotinamidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Hydroxylamine HCl | HCID 21645 | — |
| Reactant | 6-Methylpyridine-3-carbonitrile | HCID 281995 | — |
| Product | N-Hydroxy-6-methyl-nicotinamidine | HCID 73867086 | — |
Reaction Steps
1.0 g (8.5 mmol) of 6-methylpyridine-3-carbonitrile, 882 mg (12.7 mmol) of hydroxylammonium chloride and 1.4 ml (10.2 mmol) of triethylamine were reacted according to the General Method 5A. Yield: 1.11 g (87% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-cf5a47a420aa41459086e065e568fea2 |
| Source note | uspto-grants-2012_02 |