HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4'-fluoroacetophenone → HCID 58002272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4'-fluoroacetophenone | HCID 120248 | — |
| Reactant | 1-(Morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide | HCID 58002319 | — |
| Product | HCID 58002272 | HCID 58002272 | — |
Reaction Steps
100 mg (0.152 mmol) of 1-(morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide (Example 53A) and 32 mg (0.182 mmol) of 2-chloro-1-(4-fluorophenyl)ethanone were reacted according to the General Method 3. Yield: 30 mg (39% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-72327cc75e00465ea113bdeb81ed6c40 |
| Source note | uspto-grants-2012_02 |