HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorophenacyl bromide → HCID 58002456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Reactant | 1-(Morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide | HCID 58002319 | — |
| Product | HCID 58002456 | HCID 58002456 | — |
Reaction Steps
100 mg (0.224 mmol) of 1-(morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide (Example 53A) and 63 mg (0.269 mmol) of 2-bromo-1-(4-chlorophenyl)ethanone were reacted according to the General Method 3. Yield: 15 mg (12% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-d2f18a576b944d238079294890bbb3c1 |
| Source note | uspto-grants-2012_02 |