HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 58002284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 1-(Morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide | HCID 58002319 | — |
| Product | HCID 58002284 | HCID 58002284 | — |
Reaction Steps
42 mg (0.064 mmol) of 1-(morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide (Example 53A) and 15 mg (0.077 mmol) of 2-bromo-1-phenylethanone were reacted according to the General Method 3. Yield: 11 mg (34% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-8a02aa1f3e3d443cb94287d7aa533f08 |
| Source note | uspto-grants-2012_02 |