HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-2',5'-dimethoxyacetophenone → HCID 58002643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-2',5'-dimethoxyacetophenone | HCID 70997 | — |
| Reactant | 1-(Morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide | HCID 58002319 | — |
| Product | HCID 58002643 | HCID 58002643 | — |
Reaction Steps
100 mg (0.152 mmol) of 1-(morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide (Example 53A) and 49 mg (0.182 mmol) of 2-bromo-1-(2,5-dimethoxyphenyl)ethanone were reacted according to the General Method 3. Yield: 20 mg (24% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-88ff0b74bac64209815e4a308173ad2d |
| Source note | uspto-grants-2012_02 |