HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromopinacolone → HCID 58002575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromopinacolone | HCID 21642 | — |
| Reactant | 1-(Morpholin-4-ylcarbonyl)-5-[4-(trifluoromethyl)phenyl]piperidine-3-carbothioamide | HCID 58002319 | — |
| Product | HCID 58002575 | HCID 58002575 | — |
Reaction Steps
250 mg (about 0.211 mmol) of the compound from Example 53A and 154 mg (0.710 mmol) of 1-bromo-3,3-dimethylbutan-2-one were reacted according to the General Method 3. Yield: 88 mg (29% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-c118eb1763f946019fafdf977af755f9 |
| Source note | uspto-grants-2012_02 |