HCID 85773171, compound → HCID 25070766, compound

Participants

Reaction Steps

To a mixed solution of 2,2-bis(3,5-diisopropyl-4-hydroxyphenylthio)propane (500 mg, 1.09 mmol) in dichloromethane (5 mL) and hexane (5 mL) was added manganese dioxide (500 mg). The mixture was stirred for 4 hours and then filtered by using a celite, and the resulting filtrate was concentrated. Hexane was added to the residue, and the mixture was stored in a refrigerator. The generated solid was separated by a filtration, washed with hexane, and then dried to synthesize an, objective compound.

Provenance & Evidence