HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 66756276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 66756408 | HCID 66756408 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 66756276 | HCID 66756276 | — |
Reaction Steps
2.7 71.25 g of potassium carbonate are added to a solution of 75 g of methyl 2,4-dihydroxy-5-(N-methyl-N-propylsulfamoyl)benzoate in 800 ml of acetonitrile. 60 ml of benzyl bromide are subsequently added dropwise. The mixture is refluxed for 3 hours, cooled and subjected to conventional work-up. HPLC gives 113 g of methyl 2,4-dibenzyloxy-5-(N-methyl-N-propylsulfamoyl)benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119795B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-032ebeef043245f9995365c63358c8a5 |
| Source note | uspto-grants-2012_02 |