Sodium Hydroxide → HCID 23690481, compound

Participants

Reaction Steps

When the reactor contents had reached 30° C., the carbon disulfide feed was started at a slow drop-wise rate. After five minutes the sodium hydroxide feed was also started at a slow drop-wise rate. The feeds were regulated such that the reaction temperature did not exceed 45° C., and both additions were complete after approximately forty-five minutes. The reaction was then allowed to cook for one hour at 40° C., after which the 4-(3-aminopropyl)morpholine dithiocarbamate solution was a clear orange solution. The pH was 12.0-14.0 and the activity was 28-30% by calculation.

Provenance & Evidence