3-Pentanamine → 3-chloro-4-methoxy-N-(pentan-3-yl)benzamide

HRID 1644058Notes

Reaction equation

[CH3:1][CH2:2][CH:3]([NH2:6])[CH2:4][CH3:5].[Cl:7][C:8]1[CH:9]=[C:10]([CH:14]=[CH:15][C:16]=1[O:17][CH3:18])[C:11](O)=[O:12]>>[Cl:7][C:8]1[CH:9]=[C:10]([CH:14]=[CH:15][C:16]=1[O:17][CH3:18])[C:11]([NH:6][CH:3]([CH2:4][CH3:5])[CH2:2][CH3:1])=[O:12]

Participants

Reactant 2

HCID 120193-Pentanamine

HCID 1699823-Chloro-p-anisic acid

Product 1

HCID 569208383-chloro-4-methoxy-N-(pentan-3-yl)benzamideYield 40%

Procedure

Prepared in a similar manner to example 4 using 3-pentylamine and 3-chloro-4-methoxy benzoic acid. Yield 40%. MS (M+H, 256.20).

Sources & evidence

ORD record: ord-d1a5e4eddcf14a8b81732236bf1a1ef1
Source dataset: uspto-grants-2012_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08124121B2

Reaction notes

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