HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Leucine, methyl ester → HCID 57527860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Leucine, methyl ester | HCID 89967 | — |
| Reactant | 2,6-Dimethoxyisonicotinic acid | HCID 235752 | — |
| Product | HCID 57527860 | HCID 57527860 | — |
Reaction Steps
Prepared in a similar manner to example 4 using 2,6-Dimethoxy-isonicotinic acid and D-leucine methyl ester. 1H NMR (500 MHz, CDCl3): δ 0.92 (d, 3H, J=7.27 Hz), 0.93 (d, 3H, J=7.26 Hz), 1.41-1.58 (m, 8H), 3.95 (s, 3H), 4.08 (s, 3H), 4.15 (m, 1H), 6.43 (d, 1H, J=8.32 Hz), 7.47 (m, broad, 1H), 8.41 (d, 1H, J=8.34 Hz). MS (M+H; 311).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124121B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-43598e6882a042adb56a8fa691ac7662 |
| Source note | uspto-grants-2012_02 |