HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cycloheptylamine → N-cycloheptyl-2,3,5,6-tetrafluoro-4-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cycloheptylamine | HCID 2899 | — |
| Reactant | p-Toluic acid, 2,3,5,6-tetrafluoro- | HCID 69548 | — |
| Product | N-cycloheptyl-2,3,5,6-tetrafluoro-4-methylbenzamide | HCID 57527795 | — |
Reaction Steps
Prepared in a similar manner to Example 162 using cycloheptylamine and 2,3,5,6-tetrafluoro-p-toluic acid (94%). 1H NMR (CDCl3) δ 1.53 (m, 6H), 1.57 (m, 4H), 2.03 (m, 2H) 2.28 (m, 3H), 4.17 (m, 1H), 5.85 (bs, 1H). MS (304.1, M+H) m.p. 164-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124121B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-b7078b93ff66459783f1fc069730c4b1 |
| Source note | uspto-grants-2012_02 |